AFM University Introduction to Atomic Force Microscopy by Paul West

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« Chapter 1
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 « Chapter 4
 
4.1 Topography Modes
4.1.1 Contact Modes
4.1.2 Vibrating Modes
4.2 Field Modes
4.2.1 Electric Force Microscopy
4.2.2 Magnetic Force Microscopy
4.3 Material Sensing Modes
4.3.1 Lateral Force / Frictional Force
4.3.2. Vibrating Phase
4.4 Electrical Modes
4.4.1 Parametric Testing (I/V and C/V)
4.4.2 SHARK
4.4.3 Ferroelectric / Piezoelectric Testing
4.4.4 Kelvin Probe (SKPM)
4.4.5 Scanning Capacitance
4.5.1 Voltage
4.5.2 Scratching
4.5.3 Chemical Deposition
4.6 Mechanical Measurements
4.6.1 Force / Distance Curves
4.6.2 Nano Indenting
4.6.3 Frictional Measurements
4.7 Thermal Measurements
4.8 Other Modes
4.8.1 Electrochemistry
4.8.2 Scanning Tunneling Microscope
4.8.3 Pulsed Force Mode
4.8.4 Nano-Manipulation
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« Appendix A
« Appendix B
« Appendix C
« Appendix D
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Chapter 4


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Although the electrical modes are typically relatively simple to implement, getting reliable data is problematic. There are three problems:
  • The measurements are typically made on materials that are coated with contamination, and getting a reliable electrical contact is difficult.
  • If the probe is coated with a metal, the metal coating can be removed when the probe contacts the surface.
  • An oxide layer can build up on the tip or surface making the measurement unreliable.
Figure 4-22 illustrates a probe in the proximity of a sample's surface and the layers of oxide and contamination that cause uncertainty in AFM electrical measurements. The oxide layers and contamination make it difficult to make an ohmic contact between the probe and surface.
One approach to solving issues b and c is to coat the probe with a conductive diamond coating. The diamond coating is very hard and does not oxidize; however, the coating increases the diameter of the probe significantly. Even when the probe is coated with an inert layer such as diamond, there are still potential problems for contamination.
FIGURE 4-22 Electrical measurements with the AFM require the probe to make electrical contact with the coating.
4.4.1 Parametric Testing (I/V and C/V)
An electrically conductive probe may be used directly for parametric testing (see Figure 4-23). The parametric tester is attached directly between the conductive AFM probe and the sample.

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