AFM University Introduction to Atomic Force Microscopy by Paul West

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« Foreward
« Chapter 1
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 « Chapter 4
 
4.1 Topography Modes
4.1.1 Contact Modes
4.1.2 Vibrating Modes
4.2 Field Modes
4.2.1 Electric Force Microscopy
4.2.2 Magnetic Force Microscopy
4.3 Material Sensing Modes
4.3.1 Lateral Force / Frictional Force
4.3.2. Vibrating Phase
4.4 Electrical Modes
4.4.1 Parametric Testing (I/V and C/V)
4.4.2 SHARK
4.4.3 Ferroelectric / Piezoelectric Testing
4.4.4 Kelvin Probe (SKPM)
4.4.5 Scanning Capacitance
4.5.1 Voltage
4.5.2 Scratching
4.5.3 Chemical Deposition
4.6 Mechanical Measurements
4.6.1 Force / Distance Curves
4.6.2 Nano Indenting
4.6.3 Frictional Measurements
4.7 Thermal Measurements
4.8 Other Modes
4.8.1 Electrochemistry
4.8.2 Scanning Tunneling Microscope
4.8.3 Pulsed Force Mode
4.8.4 Nano-Manipulation
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« Appendix C
« Appendix D
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FIGURE 4-3 Left: SEM image of standard AFM Probe. Right: SEM image of an AFM probe coated with a conductive diamond film.
4.1 Topography Modes
A force sensor in an AFM can only work if the probe interacts with the force field associated with a surface. In ambient air, the potential energy between the probe and surface is shown in Figure 4-4. There are three basic regions of interaction between the probe and surface:
  • free space
  • attractive region
  • repulsive region
FIGURE 4-4 Potential energy diagram of a probe and sample. The attractive potential is caused by the capillary forces from surface contamination.
Attractive forces near the surface are caused by a nanoscopic layer of contamination that is present on all surfaces in ambient air. The contamination is typically an aerosol composed of water vapor and hydrocarbons. The amount of contamination depends on the environment in which the microscope is being operated. Repulsive forces increase as the probe begins to "contact" the surface. The repulsive forces in the AFM tend to cause the cantilever to bend up.
There are two primary methods for establishing the forces between a probe

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